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Modern Inorganic Synthetic Chemistry

Modern Inorganic Synthetic Chemistry

Authors
Publisher Elsevier Science Publishers
Year 01/02/2017
Edition Second
Pages 808
Version other
Language English
ISBN 9780444635952
Categories Technology: general issues
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Book description

Modern Inorganic Synthetic Chemistry, Second Edition captures, in five distinct sections, the latest advancements in inorganic synthetic chemistry, providing materials chemists, chemical engineers, and materials scientists with a valuable reference source to help them advance their research efforts and achieve breakthroughs. Section one includes six chapters centering on synthetic chemistry under specific conditions, such as high-temperature, low-temperature and cryogenic, hydrothermal and solvothermal, high-pressure, photochemical and fusion conditions. Section two focuses on the synthesis and related chemistry problems of highly distinct categories of inorganic compounds, including superheavy elements, coordination compounds and coordination polymers, cluster compounds, organometallic compounds, inorganic polymers, and nonstoichiometric compounds. Section three elaborates on the synthetic chemistry of five important classes of inorganic functional materials, namely, ordered porous materials, carbon materials, advanced ceramic materials, host-guest materials, and hierarchically structured materials. Section four consists of four chapters where the synthesis of functional inorganic aggregates is discussed, giving special attention to the growth of single crystals, assembly of nanomaterials, and preparation of amorphous materials and membranes. The new edition's biggest highlight is Section five where the frontier in inorganic synthetic chemistry is reviewed by focusing on biomimetic synthesis and rationally designed synthesis. Focuses on the chemistry of inorganic synthesis, assembly, and organization of wide-ranging inorganic systems Covers all major methodologies of inorganic synthesis Provides state-of-the-art synthetic methods Includes real examples in the organization of complex inorganic functional materials Contains more than 4000 references that are all highly reflective of the latest advancement in inorganic synthetic chemistry Presents a comprehensive coverage of the key issues involved in modern inorganic synthetic chemistry as written by experts in the field

Modern Inorganic Synthetic Chemistry

Table of contents


  • Cover image

  • Title page

  • Table of Contents

  • Copyright

  • List of Contributors

  • Preface to the Second Edition

  • Chapter 1. Introduction

  • 1.1. Chemistry of Inorganic Synthesis

  • 1.2. Major Scientific Issues in Modern Inorganic Synthetic Chemistry

  • Chapter 2. High Temperature Synthesis

  • 2.1. Attainment of High Temperature: Laboratory Furnaces and Related Techniques

  • 2.2. Types of High-Temperature Synthetic Reactions and Routes

  • 2.3. High-Temperature Solid-State Reaction

  • 2.4. Preparation of Rare Earth Containing Materials

  • 2.5. Sol?Gel Process and Precursors in High Temperature Solid Synthesis

  • 2.6. Self-Propagating High-Temperature Synthesis

  • 2.7. High-Temperature Preparation of Metal Vapors and Active Molecules for Use in Cryosynthesis

  • 2.8. High Temperature Electrolysis in Molten Salt System

  • Chapter 3. Synthesis and Purification at Low Temperatures

  • 3.1. Attainment and Measurement of Low and Ultralow Temperatures

  • 3.2. Vacuum Technique and Its Applications in Inorganic Synthesis

  • 3.3. Purification and Separation of Inorganics at Low Temperatures

  • 3.4. Synthesis of Volatile Inorganic Compounds at Low Temperatures

  • 3.5. Formation of Noble Gas Compounds Under Cryogenic Conditions

  • 3.6. Freeze-Drying Synthesis

  • 3.7. Inorganic Synthesis in Liquid Ammonia

  • 3.8. Cryosynthesis of Unusual Inorganic Compounds

  • Chapter 4. Hydrothermal and Solvothermal Syntheses

  • 4.1. Foundation of Hydrothermal and Solvothermal Syntheses

  • 4.2. Functional Materials From Hydrothermal and Solvothermal Systems

  • 4.3. Hydrothermal Biochemistry

  • 4.4. Supercritical Water: A Novel Reaction System

  • 4.5. Techniques and Methods

  • 4.6. Ionothermal Synthesis

  • Chapter 5. High Pressure Synthesis and Preparation of Inorganic Materials

  • 5.1. Experimen

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